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Calcium Citrate Tetrahydrate

Category: Mineral Chelates & Salts

Ultrafine, micronized calcium citrate tetrahydrate meeting USP-NF monograph and food-grade requirements (EC 178/2002, 852/2004). The fine particle size gives fast dispersion and a smooth mouthfeel in powders, sachets, tablets, capsules, bars, gummies and dry blends. Produced by chemical synthesis (reaction, centrifugation, drying, micronizing, sieving and metal detection) under an ISO 22000 certified food-safety system valid to 24 August 2027; country of origin China. Free of the EU and FDA major allergens, gluten free, GMO free, BSE/TSE free and vegan, with no residual solvents, no sewage-sludge contact, and free of MSG, artificial flavours, colours, preservatives, yeast and rice. Not regulated for transport (DOT, ADR, IMDG, IATA). In stock in our Montréal warehouse for prompt delivery, in 15 kg packages (inner double-layer PE bags, on pallets). Certificate of analysis, specification sheet, MSDS, processing flow chart, product statements, ISO 22000 certificate and a retained sample available on request. For liquid or acidified formulations, request a trial sample first.

Technical Specifications

CAS 5785-44-4
Formula C12H10Ca3O14·4H2O
Mol. Weight 570.5
AppearanceWhite or off-white powder
Synonyms: Calcium citrate tetrahydrate, Calcium citrate (USP), Citracal, Calcium citrate (3:2) tetrahydrate, Calcium citrate tribasic tetrahydrate, Citric acid calcium salt (2:3) tetrahydrate, E333(iii)
Applications: Food Supplement Ingredients, Dietary Supplement Ingredients, Health Ingredients, Typical Medical Treatment Ingredients, Food Grade Ingredients

Specifications

Item Specification (USP-NF) Test method
Appearance White or off-white powder Visual
Identification Meets the requirements USP-NF 2021
Assay (as anhydrous, dried basis) 97.5 – 100.5% USP-NF 2021
Calcium (as is) ≥ 20.5% Titration
Fluoride ≤ 30 ppm USP-NF 2021
Acid-insoluble substances ≤ 0.2% USP-NF 2021
Loss on drying (150 °C, 4 h) 10.0 – 13.3% USP-NF 2021
Particle size, D50 ≤ 6 µm Laser particle size analyzer
Heavy metals
Heavy metals (total) ≤ 20 ppm USP <233>
Lead (Pb) ≤ 3 ppm (customized: ≤ 0.2 ppm) USP <251> / <233>, GFAAS
Arsenic (As) ≤ 1 ppm USP <211> / <233>, AFS
Cadmium (Cd) ≤ 1 ppm USP <233>, GFAAS
Mercury (Hg) ≤ 0.1 ppm USP <261> / <233>, AFS
Microbiology
Total plate count ≤ 3,000 cfu/g ISO / GB / USP
Yeast and mould ≤ 300 cfu/g ISO / GB / USP
E. coli Negative /g ISO / GB / USP
Salmonella Negative /25 g ISO / GB / USP

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